具有好的溶解性和高的热稳定性的富勒烯-苝化合物的合成
首发时间:2003-12-23
摘要:在氩气保护下,利用N-(正丁基)-N’-(4-甲酰基苯氧戊基)-1,6,7,12-四-(4-叔丁基苯氧基)-3,4,9,10-苝酰亚胺和N-甲基甘氨酸产生的亚胺叶立德与富勒烯反应,合成了含富勒烯的苝化合物,用NMR、FT-IR、UV-Vis及TGA等方法对其结构和性能进行了表征和测试。研究结果表明此类化合物具有好的溶解性和高的热稳定性。
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Synthesis of a Novel Soluble and High Thermal Stable Fullerene-Perylene Dyad
Abstract:A novel good soluble and high thermal stable fullerene-perylene dyad, in which a perylene moiety is attached to C60, has been prepared by 1,3-dipolar cycloaddition of the azome- thine ylides generated in situ from the aldehyde and N-methylglycine and characterized by NMR, FT-IR, TGA, UV-Vis absorption and fluorescent spectra etc.
Keywords: Fullerene, Perylene, Solubility, Synthesis, Characterization
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No.1094761072119506****
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