利用自制设备合成原位Al3Fe增强铝基复合材料工艺探究
首发时间:2011-12-23
摘要:铝基复合材料具有密度低、比强度和比刚度高、耐磨性好、良好的导热、导电性及尺寸稳定等优点, 在航空航天和汽车制造等行业中有着广阔的应用前景。然而,高昂的生产成本一直限制着铝基复合材料的广泛应用。本次实验旨在探究利用简单的仪器设备合成性能良好的Al3Fe增强铝基复合材料的加工工艺,实现生产的经济性。根据实验需要,我们自制了一套自浇注式坩埚熔炼设备,该设备具有体积小,方便灵活,自动化程度高等特点,能完成从加热、保温、搅拌到浇注一系列实验过程。实验中选用的基体材料为工业纯Al,Fe元素是通过向纯Al熔体中添加由Fe粉、Mg粉及混合添加剂(主要成分为冰晶石)按比例混合并压制而成的预制压块的方式加入,之后通过机械搅拌达到Fe元素在Al基体中的均匀分布。通过金相组织观察,能谱(EDS)分析及X射线衍射(XRD)分析等手段,研究了反应温度,Fe粉的预处理和复合材料重熔工艺对最终Al3Fe增强铝基复合材料组织的影响。结果表明:850℃为较合理的反应温度,Fe粉是否进行预处理对组织影响不大,650℃重熔工艺能够很好的细化Al3Fe增强相。
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Exploration on Process to Compound Situ Al3Fe Enhanced Al Matrix Composite Material with Self-made Equipment
Abstract:Al matrix composite materials have wide application prospects for their outstanding performance, such as low density, high strength and stiffness, good abrasion performance, favorable electrical and thermal conductivity, nice dimensional stability. However, expensive production cost astricts the application of the Al matrix composite materials. This research aims to explore a process to compound Al matrix composite materials with good performance using simple equipment and to reduce the production cost. According to the experiment requirement, We make a crucible melting and automatic casting equipment which is small in size, convenience and has high automaticity. This equipment can realize the all experiment procedure including heat up, heat preservation, rabbling and pouring. The matrix material of the experiment was commercial purity aluminium. Fe in the alloy is added by precast blocks which are mixed in proportion with Fe powder and cryolite into Al melt. Mechanical rabbling can make the distribution of Fe in Al matrix more uniform. The effects of reaction temperature, the pretreatment of Fe power and remelting treatment on microstructure of final Al3Fe are analysed by optical microscopy, EDS and XRD. The results shows that the optimal reaction temperature is 850℃,the pretreatment of Fe power has weak effect on final microstructure of Al3Fe, the remelting treatment can refine the Al3Fe well.
Keywords: composite material Al Al3Fe microstructure production process
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