Mg-Zn-Y-Nd合金微细管材及血管支架的加工
首发时间:2017-05-12
摘要:镁合金由于具有良好的生物相容性和可降解性能被认为是最有潜力的支架材料之一,然而镁合金的室温塑性变形能力较差是制约微细管材制备的关键因素之一,关于血管支架的激光切割研究相对较少。本文通过热挤压得到直径3.2mm、壁厚0.4mm的管坯,然后进行多道次的长芯杆拉拔,通过对中间退火工艺的研究,最后加工出长度达到80mm,直径2.0mm、壁厚0.15mm的微细管,拉伸试验结果显示微细管的强度达到298MPa,伸长率为20%。采用80-85W的激光加工时峰值功率和较大的切割速度,切口附近基体组织基本没有变化的同时保证了支架连接筋附近的表面质量,以磷酸为主要成分的电解抛光液适用于Mg-Zn-Y-Nd合金支架的抛光,抛光过后的支架光亮,表面质量较好,不易过腐蚀。微细管及其血管支架的成功制备加快了镁合金在心血管疾病的临床应用。
关键词: Mg-Zn-Y-Nd合金 微细管材 血管支架 激光切割 电解抛光
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The processing of Mg-Zn-Y-Nd alloy micro-tubes and vascular stent
Abstract:Magnesium alloy is considered to be one of the most promising stentmaterials because of its good biocompatibility and degradability. However, the poor plasticity of magnesium alloy at room temperature is one of the key factors that restricting the preparation of micro-tubes and the research about laser cutting is relatively small.In this paper, tube blank with diameter of 3.2mm and wall thickness of 0.4mm was obtained by hot extrusion, then micro-tubes with diameter of2.0mm, wall thickness of 0.15mm and length of 80mm was fabricated by long mandrel drawing andthe intermediate annealing process. Tensile test resThe processing of Mg-Zn-Y-Nd alloy micro-tubes and vascular stentults show that the strength and elongation of micro-tubesafter annealing reach 298MP and 20%, respectively.It's appropriate to select 80-85W as the peak power during the cutting processing and use a large cutting speed to ensure the surface quality of the strut near, at the same time, the matrix microstructure near incision has not changed. Phosphoric acid as a main component is more suitable for electrolytic polishing of Mg-Zn-Y-Nd alloy stent. After electrolytic polishing, the stents' surface quality is better and looks bright, there is no over-etching. The successful preparation of micro-tubes and its vascular stents has accelerated the clinical application of magnesium alloys in cardiovascular disease.
Keywords: Mg-Zn-Y-Nd alloy micro-tubes vascular stents laser cutting electrolytic polishing
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