甘油对凝胶珠干燥成型的增塑作用研究
首发时间:2019-01-03
摘要:凝胶珠在干燥成型过程中存在结构易塌陷、质构硬化等问题,本文比较了不同干燥方法对液芯式薄荷油凝胶珠的形貌、包埋特性的影响,重点考察了甘油的添加对凝胶珠干燥成型后质构及包埋效果的调节作用,借助低场核磁和傅里叶红外光谱分别研究了凝胶珠中的水分分布情况以及添加甘油前后凝胶膜的官能团变化。结果表明,真空干燥后凝胶珠的形貌饱满,在壁材中辅以甘油后,凝胶珠的硬度从1719.5 g骤降至536.9 g,柔韧性增强,而凝胶珠的载量仍高于35%。低场核磁成像和弛豫结果显示适量的甘油能够延缓干燥过程中凝胶膜的失水,改善凝胶珠形态,提高结合水的比例。凝胶膜中海藻酸盐与甘油之间存在氢键相互作用,具有良好的增塑性,这有利于提高凝胶珠在干燥过程中的稳定性。
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Effect of glycerol on plasticization of dried gel beads
Abstract:Structural collapse and texture hardeningare easy to happen during the drying process of gel beads.Thisstudyinvestigatesthe influence of different drying methods and addition of glycerol on the morphology,encapsulation characteristics and texture of core-shell peppermint oilgel beads.The waterdistribution in the gel beads and the changes of functional group in the gel membrance before and after the addition of glycerol are investigated by low field nuclear magnetic(LF-NMR) and fourier infrared spectroscopy, respectively.The results show that the morphology and properties of gel beads are better after vacuum drying. The hardness of the gel beads with glycerolis suddenly reduced from 1719.5 g to 536.9 g, the flexibility of which is enhanced, and the loading efficiency of gel beads still higher than 35%.In addition, the results of low field nuclear magnetic indicate that glycerol can delay the dehydration of the gel menbrance during drying process,improve the morphology of the gel beads, and affect the water distribution of the dried gel beads.The hydrogen bond interaction is found between sodium alginate and glycerolin the gel membrance, which means glycerol has good plasticity and is beneficial to improve the stability of gel beads during the drying process.
Keywords: gel bead dry glycerol plasticization
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