<强流脉冲电子束诱发相变对Zr-17Nb合金微观组织及力学性能的影响>
首发时间:2020-07-28
摘要:本文主要研究了强流脉冲电子束处理对经固溶时效处理得到的双相Zr-17Nb合金(STAG)的表面组织及性能的影响。XRD结果表明:随脉冲次数的增加,αZr相沉淀开始逐渐溶解,经共析反应出现β(Zr+Nb)相以及Nb相,并发生相变 β(Zr,Nb)→ αZr + Nb。微观组织形貌分析结果表明:电子束诱发的相变过程中发生了活性共析转变,并产生了层片状珠光体组织,且其依附于等轴晶伸长,具有明显的方向性。显微硬度性能检测表明:由于电子束处理后表面的严重挤压变形,5次脉冲处理后显微硬度显著下降。15次、30次脉冲处理后由于基体发生了共析反应,生成质地较软的Nb相,使得硬度进一步下降。摩擦系数性能检测表明:15次脉冲处理后表面摩擦系数显著下降,耐磨性提高,这归因于合金表面重熔使得表面更加光滑,熔坑密度得到有效降低。
关键词: Zr-Nb合金 强流脉冲电子束 固溶时效处理 相变 表面改性
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Abstract: In this study, the effect of high-current pulsed electron beam treatment on the surface structure and properties of the dual-phase Zr-17Nb alloy (STAG) obtained by solution aging treatment were investaged. The XRD results show that the original αZr phase precipitates gradually dissolve and undergo phase change with the increase of the number of pulses, and β (Zr+Nb) phase and Nb phase appear after eutectoid reaction. The microstructure morphology analysis results show that the active eutectoid transformation occurs during the phase transition induced by HCPEB treatment and he lamellar pearlite structure is produced, it is attached to the equiaxed crystal elongation and has obvious directionality. The microhardness performance test showed that the microhardness decreased significantly after 5 pulses due to the severe extrusion deformation of the surface after the HCPEB treatment. After 15 and 30 pulse treatment, the eutectoid reaction of the matrix occurred, and resulting in a softer Nb phase, which further reduced the hardness. The friction coefficient performance test showed that the surface friction coefficient decreased significantly after 15 pulse treatments, and the wear resistance increased, which can be attributed to the remelting phenomenon of the alloy surface
Keywords: Zr-Nb alloy High current pulsed electron beam solution aging treatment phase transformation surface modification
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<强流脉冲电子束诱发相变对Zr-17Nb合金微观组织及力学性能的影响>
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