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刘刚
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期刊论文
Solid-Phase Synthesis of O-Glycosylated Nr-Fmoc Amino Acids and Analysis by High-Resolution Magic Angle Spinning NMR
J. Comb. Chem. 2004, 6, 214-219，-0001，（）：
Direct O-glycosylation of amino acids bound to TentaGel resin with a number of glycosyl trichloroacetimidate donors results in high yields. The glycosylation reaction can be easily monitored by analyzing the beadbound amino acids with high-resolution magic angle spinning (HR-MAS) NMR. These studies pave a new way for the construction of "one-bead one-compound" O-glycopeptide libraries with standard amino acid building blocks and appropriate glycosyl trichloroacetimidate donors.
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