尹衍升
目前主要从事无机材料的复合化、超细化研究,特别侧重于抗海洋微生物附着材料、近海污染物高效吸附降解材料等领域的制备科学和工艺及开发研究。
个性化签名
- 姓名:尹衍升
- 目前身份:
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学术头衔:
博士生导师
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学科领域:
材料科学基础学科
- 研究兴趣:目前主要从事无机材料的复合化、超细化研究,特别侧重于抗海洋微生物附着材料、近海污染物高效吸附降解材料等领域的制备科学和工艺及开发研究。
尹衍升,男,1956年4月山东胶南生人。多年来一直从事材料加工与新材料的教学研究的第一线工作,在材料科学研究中做了一些创新性的工作。较好的把握了材料加工与材料科学前沿新的生长点。近五年来,与课题组一道,在"金属间化合物及其陶瓷复合材料的研究"等领域获得国家及省部级奖励10项,在国内外重要刊物上发表论文150余篇,其中被SCI、EI收录87篇,出版专著4部、获得或申请发明专利5项,特别是所主持的"铁铝金属间化合物/陶瓷复合材料及其制备工艺研究",2001年度获得国家发明二等奖,铸态铁铝金属间化合物研究开发获得2003年度教育部一等奖。现担任中国海洋大学材料科学与工程研究院院长、教授、海洋材料化学学科博士生导师,目前主要从事无机材料的复合化、超细化研究,特别侧重于抗海洋微生物附着材料、近海污染物高效吸附降解材料等领域的制备科学和工艺及开发研究。
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339
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尹衍升, Yin Yan Sheng a, *, Fan Run Hua a, Xie Yong Sheng b
Materials Chemistry and Physics 44(1996)190-193,-0001,():
-1年11月30日
Based on the empirical electron theory of solids andmolecules, analysis of valence electron structures is applied to the Fe3Al intermetallic compounds. The bonding complex model of the DO3 cell is set up. Some preliminary attempts at revealing the relationship between alloy composition-structure-properties and the Fe3Al alloy phase valence electron structure are prescnted.
Bond structures, Fe3Al, Valence electrons
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尹衍升, Shou-GangChen a, b, *, Yan-ShengYin a, Dao-PingWang c, Jia Lia
Journal of Crystal Growth 267(2004)100-109,-0001,():
-1年11月30日
Pure and 2 mol% yttria-doped zirconia nano-powders were synthesized via the precipitation method, using ZrOCl2
A1., Crystal structure, A1., Defect, A1., X-ray diffraction, B1., Nanomaterials, B1., Oxides
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【期刊论文】Reaction sintering fabrication of (A1N, TiN)-A1203 composite
尹衍升, Gong Hongyu, Yin Yansheng, Li Aiju, Liu Yingcai, Zhen Yuhua, Li Chunsheng
Materials Research Bulletin 37(2002)1603-1611,-0001,():
-1年11月30日
The (A1N, TiN)-A12O3 composites were fabricated by reaction sintering powder mixtures containing 10-30 wt.% (A1, Ti)-Al2O3 at 1420-1520℃ in nitrogen. It was found that the densification and mechanical properties of the sintered composites depended strongly on the A1, Ti contents of the starting powder and hot pressing parameters. Reaction sintering 20 wt.% (A1, Ti)-Al2O3 powder in nitrogen in 1520℃ for 30 min yields (A1N, TiN)-Al2O3 composites with the best mechanical properties, with a hardness HRA of 94.1, bending strength of 687 MPa, and fracture toughness of 6.5 MPa ml/2. Microstructure analysis indicated that TiN is present as well dispersed particulates within a matrix of A1203. The A1N identified by XRD was not directly observed, but probably resides at the A12O3 grain boundary. The fracture mode of these composites was observed to be transgranular.
A., Composites, A., Oxides, A., Nitrides, D., Mechanical properties
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【期刊论文】Mechanical properties of in-situ toughened Al2O3/Fe3Al☆
尹衍升, Hongyu Gong*, Yansheng Yin, Runhua Fan, Jinsheng Zhang
Materials Research Bulletin 38(2003)1509-1517,-0001,():
-1年11月30日
Mechanical properties of in-situ toughened Al2O3/Fe3Al nano-/micro-composites were measured. Effects ofFe3Al content, sintering temperature and holding time on properties and microstructure of the composites wereinvestigated. The addition of Fe3Al nano-particles decreased the aspect ratio and grain size of Al2O3, and changedthe fracture mode of composites. The maximum bending strength and fracture toughness were 832 MPa and 7.96 MPa m1/2, which were obtained in Al2O3/5 wt.% Fe3Al sintered at 1530 8C and Al2O3/10 wt.% Fe3Al sintered at 1600 8C, respectively. Compared to monolithic alumina, the strength increased by 132% and the toughness increased by 73%. The improvement in the mechanical properties of the composites was attributed to the change in fracture mode from intergranular fracture to transgranular fracture, the "'in-situ reinforced effect" arising from the platelet grains of Al2O3 matrix, refined microstructure by dispersoids, as well as crack deflection and bridging of intergranular and intragranular Fe3Al.
A., Intermetallic compounds, A., Oxides, A., Composites, D., Mechanical properties
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【期刊论文】Mechanical properties of Fe3Al/Al2O3 composite graded coatings
尹衍升, Yan-Sheng Yina, *, Jing-De Zhanga, Jia Lia, b, Yun Chena
Applied Surface Science 221(2004)384-391,-0001,():
-1年11月30日
On the basis of analyzing the formation mechanism of thermal stress in coatings, according to practical thermal conditions and mechanical principle, the calculating model that can estimate thermal stress of coatings during fabricating process is established. Through observing the microstructure of coatings by SEM, the thermal mechanical behavior and its effect on the properties of coatings are studied. The results show that, in graded coatings, parameters of thermal mechanical behavior and fabrication stress change with the compositions. The largest stress exists in the bottom layer and the thermal stress decrease from the substrate to the surface. In graded coatings, the highest stress and the average stress are both lower in coatings. The gradient distribution of coatings' composition can effectively reduce thermal stress during fabrication process.
Fe3Al, Al2O3, Graded coating, Mechanical properties
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【期刊论文】Fabrication and properties of Fe3Al-Al203 graded coatings
尹衍升, Jingde Zhang, Yansheng Yin, Jing Li, Hong Zhang
Journal of Materials Processing Technology 134(2003)206-209,-0001,():
-1年11月30日
Fe3Al intermetallic-A12O3 ceramic graded coatings were produced by plasma spray. The microstructure and composition distribution were studied by techniques including metallurgical microscope, SEM, XRD and electron probe. The adhesive strength, micro-hardness and thermal-shock resistance of the coatings were also tested. The results showed that although the compositions of graded coatings were designed gradient transition, the composition and structure varied continuously and there were no abrupt structure changes and macro-interfaces. The structure of graded coatings exhibited macro-inhomogeneity and micro-continuity. The gradient distribution of coating composition improved adhesive strength and thermal-shock resistance of the coatings. The highest micro-hardness of coatings was obtained in the composition area of containing 75 wt.% A1203. The weakest point of the substrate-coating system was the interface between the substrate and the coating.
Intermetallic, Ceramic, Coating, Plasma spray
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【期刊论文】Fabrication and microstructure of in situ toughened Al2O3/Fe3Al
尹衍升, Hongyu Gong*, Yansheng Yin, Xin Wang, Yingcai Liu
Materials Research Bulletin 39(2004)513-521,-0001,():
-1年11月30日
Fe3Al nano-particles and commercial purity Al2O3 powders were used as raw materials to fabricate in situ reinforced Al2O3/Fe3Al nano/micro-composites. Densification and microstructure were studied. The Al2O3 matrix grains were characterized by platelet grains. The Fe3Al particles inhibited the grain growth of Al2O3 grains and limited the densification of the composites. In Al2O3/Fe3Al composites, the Fe3Al particles were uniformly dispersed in the Al2O3 matrix. The major Fe3Al micro-particles, about 1 mm in average size, existed at Al2O3 grain boundaries, and the Fe3Al nano-particles were found embedded in the matrix grains. The grain size of the intragranular particles ranged from several to several hundred nanometers. The grain size and aspect ratio of Al2O3 platelet grains and distribution of intragranular Fe3Al could be optimized by controlling the Fe3Al contents and sintering process. The in situ formed Al2O3 platelet grains, as well as Fe3Al dispersoids, were beneficial to the increase of the mechanical properties of alumina.
A., Intermetallic compounds, A., Oxides, A., Composites, D., Microstructure
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尹衍升, Shou-Gang Chena, *, Yan-Sheng Yina, Dao-Ping Wangb
Journal of Molecular Structure 690(2004)181-187,-0001,():
-1年11月30日
Nanometer zirconia powders were prepared by the precipitation method at different pHs and different reaction temperatures. X-ray results show that monoclinic zirconia is favored at pH 4 while tetragonal zirconia is favored at pH 9.5 at room temperature, and monoclinic zirconia is also favored at pH 9.5 and 70℃ reaction temperature, with the slow addition of alkali. Four models of zirconium complexes were applied to simulate the structural monomers in different pH solutions. Geometric parameters and Mulliken charge population were calculated by optimizing these complexes using the density functional theory (DFT/B3LYP). Theoretical analyses show that if Model I ([Zr(OH)2(H2O)4]2þ monomers) is favored in the aqueous precursor solution, it will be preferentially polymerized into monoclinic precursor structure irrespective of slow or quick alkali addition. Contrarily, if Model IV ([Zr(OH)7]32 monomers) is major in the aqueous precursor solution, tetragonal precursor structures are favored irrespective of slow or quick alkali addition. When Model II ([Zr(OH)4(H2O)2]0 monomers) and Model III ([Zr(OH)6]22 monomers), respectively, predominate in the aqueous precursor solution, they will be preferentially polymerized into tetragonal precursor structure at slow alkali addition, however, for quick alkali addition, they will be preferentially polymerized into monoclinic precursor structure. Our theoretical models well explain the present experimental results as well as previous experimental results, and allow building up a correlation between aqueous precursor structures and crystalline phases of zirconia.
Zirconia, Precipitation, X-ray diffraction, Density functional theory/, B3LYP, Mulliken charge population
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【期刊论文】Analysis of valence electron structures (VES) of intermetallic Fe3Al compounds
尹衍升, Yin Yansheng a, Wang Wen Xiang b, Shi Zhongliang c
Materials Chemistry and Physics 39(1995)243-247,-0001,():
-1年11月30日
Based on the empirical electron theory of solids and molecules, analysis of valence electron structures is made on Fe3Al intermetallic compounds. The bonding complex model of the DO3 cell is set up. Some preliminary attempts to discover the relationship between alloy composition, structure and properties and the Fe3Al alloy phase valence electron structure are presented.
Valence electrons, Intermetallic compounds, Bonding complexes
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【期刊论文】An initial study on SiCw-reinforced Al2 TiO5 composites
尹衍升, Yujun Zhang*, Yansheng Yin
Materials Letters 46(2000)147-148,-0001,():
-1年11月30日
The paper contains the results of a preliminary study of SiCw-reinforced Al2TiO5 matrix composites. With the increase in the SiC whisker content, the bending strength of composites also increased. For the 7 wt.% SiCw composition, the strength had increased by 170% from the value for Al2TiO5ceramic without notable alteration of thermal expansion coefficient.
Strengthened aluminum titanate, SiC, Whiskers
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