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顾宁, Ning Gu, a), Chang-an Li, Long Sun, Zhan-hui Liu, Yong-kang Sun, and Li-na Xu
,-0001,():
-1年11月30日
A dynamic chemical etching method based on siphon principle has been developed for controllable fabrication of fiber nano-tips, which could be used in near-field optical microscope and optical nanosensors. Compared with traditional static chemical etching, this method has advantages such as reproducibility, controllability, convenience, less cost, and making tip surface smooth. The overall shape and the tape angle of the tip can be effectively controlled through the speed and direction of water flux. Tips with taper angles from 20
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顾宁, Yongkang Sun, Lei Duan, Zhirui Guo, Yun DuanMu, Ming Ma, Lina Xu, Yu Zhang, Ning Gu*
Journal of Magnetism and Magnetic Materials 285(2005)65-70,-0001,():
-1年11月30日
This paper describes an improved approach for the coating of superparamagnetic magnetite nanoparticles with shells of amorphous silica. Magnetite (Fe3O4) nanoparticles are prepared by partial reduction coprecipitation method and modified by adding citric acid. The silica coating is conveniently controlled by a dilute silicate solution pretreatment and subsequent Stober process directly in ethanol. Transmission electron microscopy, photon correlation spectroscopy and zeta-potential analysis results show that the attractions between the superparamagnetic nanoparticles are screened by the silica coating. With enough tetraethylorthosilicate added, the stable core-shell colloid was obtained. Vibrating sample magnetometer characterization shows that the magnetic core-shell structure is superparamagntic.
Magnetite, Nanoparticles, Core-shell, Superparamagnetic
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