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王磊, Lei Wang, *a, b Pinhua Li, a Yuanyuan Xie, a Yanbin Ding a
Synlett 2003, No.8, 1137-1140,-0001,():
-1年11月30日
An unexpected samarium metal mediated chemoselective debromination and reduction of 1,1-dibromo-1-alkenes in methanol has been developed, which generates vinyl monobromides, alkenes, and alkanes respectively with appropriate molar ratio of samarium to 1,1-dibromo-1-alkene.
samarium metal,, 1,, 1-dibromo-1-alkenes,, debromination,, reduction,, methanol
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王磊, Lei Wang, b, * Pinhua Li a and Li Zhou a
Tetrahedron Letters Pergamon 43(2002)8141-8143,-0001,():
-1年11月30日
A novel metallic samarium promoted reduction of sodium alkyl thiosulfates in the absence of an activating agent occurs to afford the corresponding disulfides with good yields in water at 90℃.
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王磊, Pinhua Li, Lei Wang, , Yaner Yang, Xinhua Sun, Min Wang, and Jincan Yan
Heteroatom Chemistry Volume 15, Number 5, 2004,-0001,():
-1年11月30日
A novel reduction of sodium alkyl thiosulfates with InCl3(cat.)/Sm(0) system in aqueous media has been developed, which generates the corresponding disulfides in good yields.
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王磊, WANG, Lei*, a, b, LI, Pin-Hua a
CHINESE JOURNAL OF CHEMISTRY 2003, 21, 710-713,-0001,():
-1年11月30日
A microwave-enhanced, solventless Mannich condensation of terminal alkynes, primary amines with paraformaldehyde on cuprous iodide doped alumina has been investigated. The struc-tures of products depend on the ratio of alkyne to amine and paraformaldehyde.
Mannich condensation,, terminal alkyne,, paraform-aldehyde,, primary amine,, coprous iodide,, alumina,, solvent free,, microwave irradiation
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【期刊论文】The Sonogashira coupling reaction catalyzed by ultrafine nickel(0) powder
王磊, Lei Wang, *a b Pinhu a Lia and Yicheng Zhang a
Chem. Commun., 2004, 514-515,-0001,():
-1年11月30日
The Sonogashira coupling reaction catalyzed by ultrafine nickel(0) powder has been developed; terminal alkynes couple with aryl, alkenyl iodide and aryl bromide in the presence of cuprous iodide, triphenylphosphine, potassium hydroxide and ultrafine particle nickel(0) to provide the corresponding crosscoupling products with high yields.
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