Three kinds of SiC particulates (SiCp), whose diameters range from millimeter through micrometer to nanometer (designated as m-SiCp, m-SiCp and n-SiCp, respectively), were separately incorporated into an Al–6wt.%Ti–6wt.%Nb alloy by high energy ball milling. The as-milled composite particles are appreciably refined particularly when finer SiC particulate was added, and so do the in situ formed Al3Ti, AlNb2 dispersoids as well as the Nb particles. The room temperature strength and ductility of the composites, except for the stiffness, deteriorate unexpectedly. Nonetheless, elevated temperature strength and thermal stability of the composites are improved and greater strength over that of the Al–6Ti–6Nb matrix alloy is exhibited above 240°C. The changes of the mechanical properties from room to elevated temperature are correlated with the microstructure and fractographs.