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期刊论文

Reaction sintering fabrication of (A1N, TiN)-A1203 composite

尹衍升Gong Hongyu Yin Yansheng Li Aiju Liu Yingcai Zhen Yuhua Li Chunsheng

Materials Research Bulletin 37(2002)1603-1611,-0001,():

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摘要/描述

The (A1N, TiN)-A12O3 composites were fabricated by reaction sintering powder mixtures containing 10-30 wt.% (A1, Ti)-Al2O3 at 1420-1520℃ in nitrogen. It was found that the densification and mechanical properties of the sintered composites depended strongly on the A1, Ti contents of the starting powder and hot pressing parameters. Reaction sintering 20 wt.% (A1, Ti)-Al2O3 powder in nitrogen in 1520℃ for 30 min yields (A1N, TiN)-Al2O3 composites with the best mechanical properties, with a hardness HRA of 94.1, bending strength of 687 MPa, and fracture toughness of 6.5 MPa ml/2. Microstructure analysis indicated that TiN is present as well dispersed particulates within a matrix of A1203. The A1N identified by XRD was not directly observed, but probably resides at the A12O3 grain boundary. The fracture mode of these composites was observed to be transgranular.

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