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【期刊论文】Preparation and dielectric properties of polyarylene ether nitriles/TiO2 nanocomposite film
刘孝波, Cao Li, Anbing Tang, Yaobang Zou, Xiaobo Liu
C. Li et al. Materials Letters 59 (2005) 59-63,-0001,():
-1年11月30日
Polyarylene ether nitriles (PENs)/TiO2 nanocomposite has been successfully synthesized through the sol–gel process; the films were characterized by FTIR, XPS, SEM and TG. The dielectric properties of the films were also measured to find that the dielectric constant of nanocomposite films increases linearly with the TiO2 weight content and reaches 6.21 at a 20 wt.% TiO2 content. The nanocomposite films have favorable mechanical and thermal properties and are not sacrificing dielectric breakdown strength compared to that of pristine polymer. © 2004 Elsevier B.V. All rights reserved.
Polyarylene ether nitriles, Nanocomposite, Titanium oxide, Dielectric property
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刘孝波, ZhiYong Qian, Sai Li, Yi He, XiaoBo Liu
ZY. Qian et al. Polymer Degradation and Stability 84 (2004) 41-47,-0001,():
-1年11月30日
A new kind of aliphatic polyetheresteramide copolymers (PEEAs) based on E-caprolactone, 11-aminoundecanoic acid, and poly (ethylene glycol) (PEG) were synthesized by melt polycondensation. The thermal and hydrolytic degradation behaviour of these copolymers was studied using FTIR, 1H-NMR, and TGA. PEG content, thickness of the test sample, and pH of degradation medium have great effect on degradation rate. The degradation rate increased with PEG content and pH, but decreased with thickness of the test sample.
Polyetheresteramide, Degradable polymer, Thermal degradation, Hydrolytic degradation, TG
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【期刊论文】In vitro release of protein from poly (butylcyanoacrylate) nanocapsules with an aqueous core
刘孝波, Sai Li, Yi He, Cao Li, Xiaobo Liu
Colloid Polym Sci (2005) 283: 480-485,-0001,():
-1年11月30日
Factors influencing the in vitro release of bovine serum albumin (BSA) from poly(butylcyanoacrylate) (PBCA) nanocapsules, such as the pH value, BSA loading, the polymeric nanocapsule walls and protein molecular weight, were investigated in detail. The BSA release rate was affected by the degradation rate of the polymeric wall and protein loading. For low molecular weight proteins, the initial burst release was faster than that of high molecular weigh proteins and got to equilibrium quickly. Sodium dodecyl sulfate–polyacrylamide gel electrophoresis results showed that BSA encapsulated within PBCA nanocapsules did not suffer covalent aggregation or fragmentation during the initial days of in vitro incubation. For nanocapsules prepared by interfacial polymerization in waterinoil microemulsions, these findings were useful as a foundation for the development of nanocapsules with desired properties.
Nanocapsules, Protein, release, Poly (, butylcyanoacrylate), , Degradation
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【期刊论文】Alkaline degradation behavior of polyesteramide fibers: surface erosion
刘孝波, Yi He, Zhiyong Qian, Hailian Zhang, Xiaobo Liu
Colloid Polym Sci (2004) 282: 972-978,-0001,():
-1年11月30日
In this work, a new kind of aliphatic polyesteramide (PEA) copolymer based on €-caprolactone and 6-aminocaproic acid was synthesized by the melt polycondensation method. Biodegradable PEA fibers were processed by the meltspinning method. 1H-NMR, FTIR, SEM, and tensile testing were used to characterize the degradation of PEA fibers in concentrated alkaline solution. The PEA fiber undergoes surface erosion in such concentrated alkaline solutions.
Polyesteramide, Degradation, Fiber, Surface, Erosion
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