Well-aligned zinc oxide whiskers with high density were successfully prepared on amorphous substrate by atmospheric metal-organic chemical vapor deposition. X-ray diffraction measurements indicated that the ZnO whiskers were wurtzite crystal structure, andgrew non-epitaxially on glass substrate along ZnO [0001] direction. ZnO whiskers with uniform distributions in their diameters and lengths grew vertically on the amorphous substrate. The effects of deposition conditions and the growth mechanism of ZnO whiskers by MOCVD were discussed. Both the growth habit andthe growth circumstance significantly affectedthe morphology of the whiskers.

采用湿化学法合成了前驱物ZrMo2O7（OH）2（H2O）2，并用SEM观察了不同回流时间所得晶粒形貌，结果显示经过较短时间的回流（12h）就能获得一定尺寸的晶粒并趋于稳定。观察了不同回流温度所得前驱物晶粒形貌，其晶粒呈长方体棒状形态，XRD结果证明结晶度随回流温度的升高而提高；探讨了不同回流温度下所获得的前驱物ZrMo2O7（OH）2（H2O）2 对合成立方ZrMo2O8的影响。结果表明，100℃回流所得前驱物经热处理后可获得纯立方相ZrMo2O8。此外，对前驱物的热处理温度选择在400℃左右有利于纯立方相的获得。

The effects of S impurities, both interstitial and substitutional, on adhesions at Al2O3/Ni and ZrO2/Ni interfaces were investigated with the first-principles method. The effects of S impurities on the adhesion of the Ni/Al2O3 interfaces are quite obvious, and changes in equilibrium adhesive energies evidently range with the type of impurities. The effects of Simpurities on the adhesion of the Ni/ZrO2 interface are very slight. For the two interfaces considered, both interstitial and substitutional S impurities will increase their equilibrium interfacial distances.

本研究是在大量的实验数据的基础上，通过建立物理、数学模型，用计算机计算模拟弯曲型驱动器的振动模式，得到了驱动器受激时的振动状况，如各阶谐振频率和各阶谐振振型等。另外还给出了各阶谐振频率的拟合经验公式。最后，计算模拟并且分析了加轴驱动器振动模态，对加轴的可行性给予了评价。

通过对磷酸铝、磷酸铬及磷酸铝磷酸铬体系进行焙烧实验，测其收缩率、孔隙率，并进行XRD物相分析，研究磷酸铝、磷酸铬及磷酸铝一磷酸铬体系烧结性能。研究结果表明，含磷酸铝70%～80%的磷酸铝-磷酸铬混合体系在1300～1400℃可烧结。